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Fundamentals of Powder Diffraction and Structural Characterization of Materials
Pecharsky (Iowa State University) and Zavalij (State University of New York, Binghamton) explain in their preface that the powder diffraction method has been used for more than 90 years as a means of structural characterization of materials; but it has become even more important to advancements in materials science, chemistry, physics, natural sciences, and engineering due to developments in the past decade such as digital x-ray recording, groundbreaking work showing the application of powder diffraction data to structure refinement and solution, and computers and the internet. This text for undergraduate and graduate students requires no prior knowledge of the subject. It provides both theoretical and practical coverage with emphasis on data collected using conventional x-ray sources and general-purpose powder diffractometers. The included CD-ROM contains color versions of some 300 illustrations as well as powder diffraction data needed for the end-of-chapter problems.
Fundamentals of nanoscale film analysis
The book describes the fundamentals of materials characterization from the standpoint of the incident photons or particles which interrogate nanoscale structures. These induced reactions lead to the emission of a variety of detected of particles and photons. It is the energy and intensity of the detected beams that is the basis of the characterization of the materials. The array of experimental techniques used in nanoscale materials analysis covers a wide range of incident particle and detected beam interactions.
Functionalized Nanoscale Materials, Devices and Systems
The primary objective of the NATO Advanced Study Institute (ASI) titled “Functionalized Nanoscale Materials, Devices, and Systems for Chem. -Bio Sensors, Photonics, and Energy Generation and Storage” was to present a contemporary and comprehensive overview of the field of nanostructured materials and devices and its applications in chem. -bio sensors, nanophotonics, and energy generation and storage devices. The study has become one of the most promising disciplines in science and technology, as it aims at the fundamental understanding of new physical, che- cal, and biological properties of systems and the technological advances arising from their exploration. Such systems are intermediate in size, between the isolated atoms and molecules and bulk material, where the unique transitional characteristics between the two can be understood, controlled, and manipulated.
Functional MRI : Basic principles and clinical applications
This practical and timely volume presents an overview of the principles of fMRI and explains key concepts, including scanning methodologies, experimental research design, and data analysis. Informative discussions cover the technical and clinical challenges associated with fMRI. A neuroanatomical atlas adds to the sensible approach and serves as a useful reference by clearly illustrating normal functioning for important areas of the brain.
Frontiers of Optical Spectroscopy ; Investigating Extreme Physical Conditions with Advanced Optical Techniques
Advanced spectroscopic techniques allow the probing of very small systems and very fast phenomena, conditions that can be considered "extreme" at the present status of our experimentation and knowledge. Quantum dots, nanocrystals and single molecules are examples of the former and events on the femtosecond scale examples of the latter. The purpose of this book is to examine the realm of phenomena of such extreme type and the techniques that permit their investigations. Each author has developed a coherent section of the program starting at a somewhat fundamental level and ultimately reaching the frontier of knowledge in the field in a systematic and didactic fashion. The formal lectures are complemented by additional seminars.
Frontiers in Chemical Sensors : Novel Principles and Techniques
With their similarity to the organs of the most advanced creatures that inhabit the Earth, sensors are regarded as being the “senses of electronics”: arti?cial eyes and ears that are capable of seeing and hearing beyond the range of - man perception; electronic noses and tongues that can recognise odours and ?avours without a lifetime training; touch that is able not only to feel the texture and temperature of the materials but even to discern their chemical compo- tion. Among the world of chemical sensors, optical devices (sometimes termed “optodes”, from the Greek “the optical way”) have reached a prominent place in those areas where the features of light and of the light-matter interaction show their advantage: contactless or long-distance interrogation, detection sensitivity, analyte selectivity, absence of electrical interference or risks, and lack of analyte consumption,
From X-ray Binaries to Quasars : Black Holes on All Mass Scales
This volume brings together contributions from many of the world's leading authorities on black hole accretion. The papers within represent part of a new movement to make use of the relative advantages of studying stellar mass and supermassive black holes and to bring together the knowledge gained from the two approaches. The topics discussed here run the gamut of the state of the art in black hole observational and theoretical work-variability, spectroscopy, disk-jet connections, and multi-wavelength campaigns on black holes are all covered.
Fluorescence Spectroscopy in Biology : Advanced Methods and their Applications to Membranes, Proteins, DNA, and Cells
This volume - the third book in the Springer-Verlag Series on Fluorescence - reviews some of the most characteristic topics of the multidisciplinary area of fluorescence applications in life sciences either presendted directly at th 8th MAF Conference or considered to be a cruical development in the field. In the initial contribution in Part 1 - Basics and Advanced Approaches, the - itors explain the basics of fluorescence and illustrate the relationship between some modern fluorescence techniques and classical approaches. The second contrigution by B.
Fluorescence of supermolecules, polymers, and nanosystems
The field of fluorescence continues to steadily grow, both in its fundamental aspects and in applications in highly interdisciplinary areas including analytical, physical and organic chemistry, molecular sciences, biology, biomedicine and medical research. The 4th volume in the Springer Series on Fluorescence focuses on the fluorescence of nanosystems, polymers and supermolecules, and the development and application of fluorescent probes. Special emphasis is placed on the fluorescence of artificial and biological nanosystems, single molecule fluorescence and the luminescence of polymers, micro- and nanoparticles and nanotubes. Fluorescence microscopy and fluorescence correlation spectroscopy are covered as well. Historical aspects of this growing field and an overview of fluorescence applications are also provided.
Fisica solare = Solar physics
An introduction to Solar Physics, intended to illustrate to those who intend to approach this discipline (students, PhDs, researchers) the physical mechanisms underlying the complex phenomena observed on our closest star. It does not claim to be exhaustive (suffice it to say that solar physics spans a wide range of disciplines, such as nuclear physics, thermodynamics, electrodynamics, atomic and molecular physics, spectroscopy across all bands of the electromagnetic spectrum, magnetohydrodynamics, plasma physics, the development of new instrumentation, optics, etc.). Rather, a number of topics of fundamental relevance to the current study of the Sun have been selected (especially with regard to ground-based observations with large telescopes), and an attempt has been made to provide a general overview of these topics, including their historical evolution, without going into excessive detail. Since Solar Physics can rightfully be considered the "Rosetta Stone" of all Astrophysics, the volume can also be considered a valid introduction to this subject.
Femtosecond laser spectroscopy
As concepts and methodologies have evolved over the past two decades, the realm of ultrafast science has become vast and exciting and has impacted many areas of chemistry, biology and physics, and other fields such as materials science, electrical engineering, and optical communication. The field has recently exploded with the announcement of a series of remarkable new developments and advances. This volume surveys this recent growth in eleven chapters written by leading international researchers in the field. It includes sections on femtosecond optical frequency combs, soft x-ray femtosecond laser sources, and attosecond laser sources. In addition, the contributors address real-time spectroscopy of molecular vibrations with sub-5-fs pulses and multidimensional femtosecond coherent spectroscopies for studying molecular and electron dynamics. Novel methods for measuring and characterizing ultrashort laser pulses and ultrashort pulses of light are also described. The topics covered are revolutionizing the fields of biomedical imaging, electron dynamics, ultrahigh precision spectroscopy, and optical frequency metrology. Surveying the latest advances in ultrafast lasers, Femtosecond Laser Spectroscopy will be of interest to both researchers and graduate students.
Femtosecond laser pulses : Principles and experiments
This is the second edition of this advanced textbook written for scientists who require further training in femtosecond science. Four years after pub- cation of the ?rst edition, femtosecond science has overcome new challenges and new application ?elds have become mature. It is necessary to take into account these new developments. Two main topics merged during this period that support important scienti?c activities: attosecond pulses are now gen- ated in the X-UV spectral domain, and coherent control of chemical events is now possible by tailoring the shape of femtosecond pulses. To update this advanced textbook, it was necessary to introduce these ?elds; two new ch- ters are in this second edition: “Coherent Control in Atoms, Molecules, and Solids”(Chap.11)and“AttosecondPulses”(Chap.12)withwell-documented references. Some changes, addenda, and new references are introduced in the ?rst edition’s ten original chapters to take into account new developments and updatethisadvancedtextbookwhichistheresultofascienti?cadventurethat started in 1991. At that time, the French Ministry of Education decided that, in view of the growing importance of ultrashort laser pulses for the national scienti?c community, a Femtosecond Centre should be created in France and devoted to the further education of scientists who use femtosecond pulses as a research tool and who are not specialists in lasers or even in optics.
Experimental Glycoscience : Glycobiology
The aim of this book is to provide experimental protocols covering many aspects of glycobiology, glycotechnology, and chemistry: biochemistry, molecular and cellular biology, genetics, physiology, and medicine. The protocols are all self-contained descriptions of the equipment and reagents needed, followed by details of the experimental procedure.
Esterification of Polysaccharides
Polysaccharide esters (cellulose and starch) are among the first polymeric materials applied commercially. The way of producing these technically relevant derivatives, mainly the carboxylic acid esters of C2 to C4 acids, have not been changed significantly during their history of manufacture. The investigation of new acylation methods and strategies of analysis was revived during the last decade by the search for tailored, biocompatible, material for specific fields of application, e.g., biotechnology, sensor technique and medicine. Unconventional solvents were developed for completely homo-geneous acylation reaction applying state of the art techniques of modern organic chemistry for polysaccharide modification. This book will provide a first comprehensive summary of acylation methods in a very practical manner. Detailed structure analysis is indispensable for the evaluation of structure-property-relationships. Spectroscopic methods in particular FTIR- and NMR spectroscopy including two dimensional methods are of increasing importance.
Essentials of pharmaceutical analysis
Provides detailed information on the background, basic principles, and components of techniques used for the analysis of pharmaceuticals and biopharmaceuticals. Focusing on those analytical techniques that are most frequently used for pharmaceuticals, it classifies them into three major sections and 19 chapters, each of which discusses a respective technique in detail. Chiefly intended for graduate students in the pharmaceutical sciences, the book will familiarize them with the components, working principles and practical applications of these indispensable analytical techniques.
Essential NMR : For Scientists and Engineers
ESSENTIAL NMR is a set of lecture notes for scientists and engineers who want to brush up on their knowledge of NMR. This book is also a compendium for graduate and postgraduate students of physics and chemistry as well as for their teachers, covering all fields of NMR, i.e. NMR methodology and hardware, chemical analysis, 2D-spectroscopy, NMR imaging, flow NMR, and quality control NMR. The material, selected and organized for a one-semester course, is presented with pairs of pages addressing particular topics. One page of each pair provides a text containing the key information, the other page shows a color illustration. This is the most comprehensive textbook on NMR to date.
ESR Spectroscopy in Membrane Biophysics
Membrane proteins offer the greatest challenge in structural biology, and there is an urgent need to develop and apply new biophysical methodologies that are able to generate detailed structural information. Among modern biophysical techniques, site-directed spin-labeling electron spin resonance (SDSL-ESR) appears to show the highest potential to further develop the field. The objective of this book is to provide in-depth information about new advances of SDSL-ESR in membrane biophysics, emphasizing recent developments in the application to membrane proteins.
Enhancing the Dissolution Rate of Atorvastatin by Solid Dispersion Technique
In the last few decades, solid dispersion (SD) technology had been studied as an approach to produce an amorphous carrier to enhance the solubility, dissolution rate, and bioavailability of poorly water-soluble drugs. The use of suitable carrier and methodology in the preparation of SDs play a significant role in the biological behavior of the SDs. Atorvastatin is a statin group HMG-CoA reductase inhibitor drug that is commonly used to adverse cardiovascular events and to lower blood total cholesterol and LDL-cholesterol. the solubility of atorvastatin in water is very low (0.1 mg mL− 1), which results in reduced bioavailability. In order to enhance its solubility, we have prepared solid dispersions (SDs) of atorvastatin at different drug: polymer ratios (1:2, 1:10, 1:20,1:25 and 1:40), using polyethylene glycol 6000 as polymer and different preparation methods (co-precipitate and melting methods) The characterization of the SDs was performed using differential scanning calorimetry (DSC), Fourier transform infrared spectroscopy (FTIR) The solubility of AT was improved by the incorporation PEG6000.
Energy dissipation in molecular systems
Energy Dissipation in Molecular Systems analyzes experimental data on the redistribution and dissipation of energy injected into molecular systems by radiation or charged particles. These processes, competing with such practically important relaxation channels as chemical reaction or stimulated emission (laser action), are the primary focus in this monograph. Among other topics, the book treats vibrational redistribution and electronic relaxation in isolated molecules and the effects of inter-molecular interactions (collisions, complex formation, solvent effects) on the relaxation paths. Primary photo-chemical processes (such as isomerization, proton or hydrogen-atom transfer, electron transfer and ionization) are also treated as particular cases of vibrational or electronic relaxation. Only a basic knowledge of quantum mechanics and spectroscopy is assumed and calculations are kept to a strict minimum, making the book more accessible to students.
EMC 2008 ; 14th European Microscopy Congress 1-5 September 2008, Aachen, Germany ; Vol.3 : Life Science
Proceedings of the14th European Microscopy Congress, held in Aachen, Germany, 1-5 September 2008. Jointly organised by the European Microscopy Society (EMS), the German Society for Electron Microscopy (DGE) and the local microscopists from RWTH Aachen University and the Research Centre Jülich, the congress brings together scientists from Europe and from all over the world. The scientific programme covers all recent developments in the three major areas of instrumentation and methods, materials science and life science.
